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Separation and preconcentration methods have also been utilised in other determination techniques. Spectrophotometric methods which are widely used for the determination of the elements in a large variety of inorganic materials are presented in the book whilst separation and preconcentration procedures combined with spectrophotometry are …
Analytical Spectroscopy Library 10 Separation, Preconcentration and Spectrophotometry in Inorganic Analysis Analytical Spectroscopy Library A Series of Books Devoted to the Application of Spectroscopic Techniques to Chemical Analysis Volume 1 NMR for Liquid Fossil Fuels, by L. Petrakis and D. Allen Volume 2 Advances …
Beiraghi et al. [18, 19] described two methods for the preconcentration and determination of beryllium by spectrophotometry based on CPE of a complex of beryllium with chrome azurol S or 1,8-dihydroxyanthrone (anthralin) in water samples using the mixed micelle mediated extraction method. A comparison of these methods with previously …
The sensitivity and stability of beryllium atomic absorption were enhanced in the presence of palladium as a matrix modifier. The detection limit (3σ) for beryllium was 0.050 ng dm−3, based on a 400-fold preconcentration using 40 cm3 of the sample water; the relative standard deviation was 1.8% (2.0 ng dm−3, n = 8).
1. Introduction. Beryllium (Be) isotopes in seawater have become a unique tool in the field of ocean sciences. The stable isotope 9 Be exists in ppq levels (5–30 pmol kg −1 [1], [2]) in seawater and is derived from the earth's crust (i.e., of lithogenic origin) via river transport to the ocean [3].The cosmogenic Be isotope 10 Be in seawater has been …
Okutani et al. [19] determined beryllium at μg L −1 levels in water samples by graphite furnace atomic absorption spectrometry (GF-AAS) after preconcentration and separation as the beryllium acetylacetone complex on activated carbon.
This step in an analytical procedure is known as a preconcentration. An example from the analysis of water samples illustrates how we can simultaneously accomplish a separation and a preconcentration. In the gas chromatographic analysis for organophosphorous pesticides in environmental waters, the analytes in a 1000-mL …
A quick, simple and effective chromatographic method for the separation of beryllium from a wide range of elements is described. The elements selected comprise elements which can interfere with the determination of beryllium by inductively coupled plasma-atomic emission spectroscopy (ICP-AES) and elements which commonly occur in …
The Separation of Beryllium from Selected Elements Using the Dipex Extraction Chromatographic Resin. September 2005. Solvent Extraction and Ion …
A simple and sensitive method is presented for solid phase extraction (SPE) and preconcentration of trace quantities of beryllium using octadecyl silica gel modifed with aurin tricarboxylic acid ...
Magnetically-assisted chemical separation/preconcentration method for the analysis of beryllium from aqueous solutions was developed. According to this method several extractants were coated on certain magnetic microparticles to assist …
Semantic Scholar extracted view of "Separation of beryllium and aluminium from other elements using an ion-exchange resin with N-benzoylphenylhydroxylamine as a functional group" by J. Das et al. ... Separation and preconcentration of ultra trace amounts of beryllium in water samples using mixed micelle-mediated extraction and determination …
The proposed method was successfully applied to the determination of beryllium in real water samples and the analytical characteristics of the method obtained, limit of detection, linear range and preconcentration factor were obtained. A cloud-point extraction process using a mixed micelle of the cationic surfactant cetyl pyridinium …
The method is based on the preconcentration of the complexes of beryllium-acetylacetone plus morin, oxine, PAN and PAR on activated carbon at different pH values. The adsorbed beryllium was eluted with aqua regia and measured by flame atomic absorption spectrometry (FAAS). Recoveries of up to 85% were achieved.
Preconcentration and separation of ultra-trace beryllium using quinalizarine-modified magnetic microparticles
Preconcentration and separation of ultra-trace beryllium using quinalizarine-modified magnetic microparticles. | Semantic Scholar. DOI: …
method for the separation and preconcentration of a number of radionuclides and metal ions from a wide range of matrices (8). The objective of this study was to evaluate the separation and preconcentration of beryllium from simulated industrial and environmental samples using an extraction chromatographic (EXC) resin called Dipex® (9).
Magnetically-assisted chemical separation/preconcentration method for the analysis of beryllium from aqueous solutions was developed. According to this method …
A rapid and simple preconcentration method by selective adsorption using activated carbon as an adsorbent and acetylacetone as a complexing agent is described for the determination of a trace amount of beryllium by graphite furnace atomic absorption spectrometry. The beryllium-acetyl-acetonate compler is adsorbed easily onto activated …
Preconcentration of beryllium via octadecyl silica gel microparticles doped with aluminon, and its determination by flame atomic absorption spectrometry. 2009 • ... (1000 ppm) was prepared methods for the separation and preconcentration of by dissolving the proper amount of BeSO4·4H2O in small amounts of Be + 2. However, most of these doubly ...
The low concentration of beryllium ions in the presence of relatively high concentration of other ions makes it difficult to directly determination of beryllium ions. …
Magnetically-assisted chemical separation/preconcentration method for the analysis of beryllium from aqueous solutions was developed. According to this method several extractants were coated on certain magnetic microparticles to assist the extraction of beryllium from the aqueous solutions.
From the preconcentration of aluminium and beryllium with chrome azurol S, enrichment factors up to 10 and 20, respectively, could be achieved. For thallium with rhodamine B the factor was 50.
PDF | On Jan 1, 2021, Kai Deng and others published Preconcentration and determination of beryllium and rare earth elements in small volumes of marine pore-water | Find, read and cite all the ...
In the present study a cloud point extraction process using mixed micelle of the cationic surfactant cetyl-pyridinium chloride (CPC) and non-ionic surfactant Triton X-114 for extraction of beryllium from aqueous solutions is developed. The extraction of analyte from aqueous samples was performed in …
It was usually used to mask the interfering ions accompanying beryllium during preconcentration, precipitation or classical separation. Addition of EDTA-2Na minimizes precipitation of aluminum, chromium and iron and further reduces co-precipitation of manganese, cobalt, nickel and zinc, via masking them during beryllium separation …
Request PDF | Cloud point extraction based on binary Surfactants for separation, preconcentration and spectrophotometric determination of beryllium with 1,8-dihydroxy anthrone | A new micelle ...
Magnetically-assisted chemical separation/preconcentration method for the analysis of beryllium from aqueous solutions was developed. According to this method several extractants were coated on certain magnetic microparticles to assist the extraction of beryllium from the aqueous solutions.
Precise measurements of such low Be concentrations thus require methods that enable the preconcentration of Be, that is, the separation of Be from the seawater matrix and its concentration into …
Because the amount of beryllium in 10 mL of sample solution is measured after preconcentration by CPE in a final volume of nearly 0.6 mL (0.2 mL surfactant-rich phase + 0.4 mL diluent), the solution is concentrated by a factor of 16.7. The improvement factor, defined as the slope ratio of the calibration graph of the CPE method to that of the ...
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